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2-Ethylhexanoate\uff09\u4f5c\u4e3a\u4e00\u79cd\u91cd\u8981\u7684\u6709\u673a\u950c\u5316\u5408\u7269\uff0c\u5176\u7269\u7406\u548c\u5316\u5b66\u6027\u8d28\u5bf9\u5176\u5728\u5404\u79cd\u5e94\u7528\u573a\u666f\u4e2d\u7684\u8868\u73b0\u81f3\u5173\u91cd\u8981\u3002\u4ee5\u4e0b\u662f\u8be5\u5316\u5408\u7269\u7684\u4e3b\u8981\u7269\u7406\u548c\u5316\u5b66\u7279\u6027\uff1a<\/p>\n<h4>\u7269\u7406\u6027\u8d28<\/h4>\n<ol>\n<li>\n<p><strong>\u5916\u89c2<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u901a\u5e38\u4e3a\u767d\u8272\u81f3\u6de1\u9ec4\u8272\u7684\u7ed3\u6676\u6027\u7c89\u672b\u6216\u6db2\u4f53\uff0c\u5177\u4f53\u5f62\u6001\u53d6\u51b3\u4e8e\u5176\u7eaf\u5ea6\u548c\u5236\u5907\u65b9\u6cd5\u3002\u9ad8\u7eaf\u5ea6\u7684\u5f02\u8f9b\u9178\u950c\u901a\u5e38\u5448\u73b0\u4e3a\u767d\u8272\u7c89\u672b\uff0c\u800c\u4f4e\u7eaf\u5ea6\u7684\u4ea7\u54c1\u53ef\u80fd\u5e26\u6709\u8f7b\u5fae\u7684\u9ec4\u8272\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u7194\u70b9<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u7684\u7194\u70b9\u7ea6\u4e3a100-110\u00b0C\uff0c\u8fd9\u4e00\u7279\u6027\u4f7f\u5176\u5728\u5e38\u6e29\u4e0b\u6613\u4e8e\u5904\u7406\uff0c\u4f46\u5728\u8f83\u9ad8\u6e29\u5ea6\u4e0b\u53ef\u80fd\u4f1a\u53d1\u751f\u76f8\u53d8\uff0c\u8fd9\u5bf9\u67d0\u4e9b\u5e94\u7528\uff08\u5982\u9ad8\u6e29\u52a0\u5de5\uff09\u63d0\u51fa\u4e86\u6311\u6218\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u6cb8\u70b9<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u7684\u6cb8\u70b9\u8f83\u9ad8\uff0c\u901a\u5e38\u5728200\u00b0C\u4ee5\u4e0a\uff0c\u8fd9\u4f7f\u5f97\u5b83\u5728\u5927\u591a\u6570\u5de5\u4e1a\u5e94\u7528\u4e2d\u8868\u73b0\u51fa\u826f\u597d\u7684\u70ed\u7a33\u5b9a\u6027\uff0c\u4e0d\u6613\u6325\u53d1\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u5bc6\u5ea6<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u7684\u5bc6\u5ea6\u7ea6\u4e3a1.1 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cP\uff0c\u8fd9\u4e00\u7279\u6027\u4f7f\u5176\u5728\u6d82\u6599\u3001\u6da6\u6ed1\u5242\u7b49\u5e94\u7528\u4e2d\u5177\u6709\u826f\u597d\u7684\u6d41\u52a8\u6027\uff0c\u4fbf\u4e8e\u52a0\u5de5\u548c\u6d82\u5e03\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u7535\u5bfc\u7387<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u7684\u7535\u5bfc\u7387\u8f83\u4f4e\uff0c\u5c5e\u4e8e\u7edd\u7f18\u6750\u6599\uff0c\u8fd9\u4f7f\u5f97\u5b83\u5728\u7535\u5b50\u5316\u5b66\u54c1\u548c\u7edd\u7f18\u6750\u6599\u4e2d\u5177\u6709\u6f5c\u5728\u7684\u5e94\u7528\u4ef7\u503c\u3002<\/p>\n<\/li>\n<\/ol>\n<h4>\u5316\u5b66\u6027\u8d28<\/h4>\n<ol>\n<li>\n<p><strong>\u70ed\u7a33\u5b9a\u6027<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u5177\u6709\u8f83\u597d\u7684\u70ed\u7a33\u5b9a\u6027\uff0c\u80fd\u591f\u5728\u8f83\u5bbd\u7684\u6e29\u5ea6\u8303\u56f4\u5185\u4fdd\u6301\u5176\u5316\u5b66\u7ed3\u6784\u4e0d\u53d8\u3002\u7136\u800c\uff0c\u5f53\u6e29\u5ea6\u8d85\u8fc7\u4e00\u5b9a\u9608\u503c\u65f6\uff0c\u5b83\u53ef\u80fd\u4f1a\u53d1\u751f\u5206\u89e3\u6216\u4e0e\u5176\u4ed6\u7269\u8d28\u53d1\u751f\u53cd\u5e94\uff0c\u751f\u6210\u526f\u4ea7\u7269\u3002\u7814\u7a76\u8868\u660e\uff0c\u5f02\u8f9b\u9178\u950c\u5728200\u00b0C\u4ee5\u4e0b\u7684\u6e29\u5ea6\u8303\u56f4\u5185\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u70ed\u7a33\u5b9a\u6027\uff0c\u4f46\u5728\u66f4\u9ad8\u6e29\u5ea6\u4e0b\u53ef\u80fd\u4f1a\u53d1\u751f\u5206\u89e3\uff0c\u751f\u6210\u6c27\u5316\u950c\u548c\u5176\u4ed6\u526f\u4ea7\u7269\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u5316\u5b66\u7a33\u5b9a\u6027<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u5728\u5e38\u6e29\u4e0b\u5316\u5b66\u6027\u8d28\u8f83\u4e3a\u7a33\u5b9a\uff0c\u4e0d\u6613\u4e0e\u7a7a\u6c14\u4e2d\u7684\u6c27\u6c14\u3001\u6c34\u5206\u7b49\u53d1\u751f\u53cd\u5e94\u3002\u7136\u800c\uff0c\u5728\u5f3a\u9178\u3001\u5f3a\u78b1\u6216\u8fd8\u539f\u6027\u73af\u5883\u4e2d\uff0c\u5b83\u53ef\u80fd\u4f1a\u53d1\u751f\u6c34\u89e3\u6216\u6c27\u5316\u53cd\u5e94\uff0c\u751f\u6210\u4e0d\u7a33\u5b9a\u7684\u4e2d\u95f4\u4f53\u6216\u7ec8\u4ea7\u7269\u3002\u56e0\u6b64\uff0c\u5728\u50a8\u5b58\u548c\u4f7f\u7528\u8fc7\u7a0b\u4e2d\uff0c\u5e94\u907f\u514d\u63a5\u89e6\u5f3a\u9178\u3001\u5f3a\u78b1\u548c\u8fd8\u539f\u6027\u7269\u8d28\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u53cd\u5e94\u6027<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u53ef\u4ee5\u4e0e\u5176\u4ed6\u91d1\u5c5e\u76d0\u3001\u6709\u673a\u9178\u3001\u80fa\u7c7b\u5316\u5408\u7269\u7b49\u53d1\u751f\u53cd\u5e94\uff0c\u751f\u6210\u65b0\u7684\u5316\u5408\u7269\u3002\u4f8b\u5982\uff0c\u5b83\u4e0e\u94dd\u3001\u9541\u7b49\u91d1\u5c5e\u76d0\u53cd\u5e94\uff0c\u53ef\u4ee5\u5f62\u6210\u590d\u5408\u91d1\u5c5e\u76d0\uff0c\u5177\u6709\u66f4\u597d\u7684\u50ac\u5316\u6027\u80fd\uff1b\u4e0e\u6709\u673a\u9178\u53cd\u5e94\uff0c\u53ef\u4ee5\u751f\u6210\u76f8\u5e94\u7684\u916f\u7c7b\u5316\u5408\u7269\uff0c\u5177\u6709\u4e0d\u540c\u7684\u7269\u7406\u548c\u5316\u5b66\u6027\u8d28\u3002\u6b64\u5916\uff0c\u5f02\u8f9b\u9178\u950c\u8fd8\u53ef\u4ee5\u4e0e\u80fa\u7c7b\u5316\u5408\u7269\u53cd\u5e94\uff0c\u751f\u6210\u9170\u80fa\u7c7b\u5316\u5408\u7269\uff0c\u8fd9\u4e9b\u5316\u5408\u7269\u5728\u6d82\u6599\u3001\u5851\u6599\u7b49\u9886\u57df\u5177\u6709\u5e7f\u6cdb\u7684\u5e94\u7528\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u6297\u6c27\u5316\u6027<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u5177\u6709\u4e00\u5b9a\u7684\u6297\u6c27\u5316\u6027\u80fd\uff0c\u80fd\u591f\u5728\u4e00\u5b9a\u7a0b\u5ea6\u4e0a\u6291\u5236\u81ea\u7531\u57fa\u7684\u751f\u6210\uff0c\u5ef6\u7f13\u6750\u6599\u7684\u8001\u5316\u8fc7\u7a0b\u3002\u8fd9\u4e00\u7279\u6027\u4f7f\u5176\u5728\u6da6\u6ed1\u5242\u3001\u5851\u6599\u3001\u6a61\u80f6\u7b49\u9886\u57df\u7684\u5e94\u7528\u4e2d\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u6297\u8001\u5316\u6027\u80fd\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u50ac\u5316\u6d3b\u6027<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u5177\u6709\u826f\u597d\u7684\u50ac\u5316\u6d3b\u6027\uff0c\u80fd\u591f\u4fc3\u8fdb\u591a\u79cd\u5316\u5b66\u53cd\u5e94\u7684\u8fdb\u884c\u3002\u4f8b\u5982\uff0c\u5728\u6d82\u6599\u4e2d\uff0c\u5b83\u53ef\u4ee5\u4f5c\u4e3a\u50ac\u5e72\u5242\uff0c\u52a0\u901f\u6cb9\u6027\u6d82\u6599\u7684\u5e72\u71e5\u8fc7\u7a0b\uff1b\u5728\u805a\u5408\u53cd\u5e94\u4e2d\uff0c\u5b83\u53ef\u4ee5\u4f5c\u4e3a\u5f15\u53d1\u5242\u6216\u94fe\u8f6c\u79fb\u5242\uff0c\u8c03\u8282\u805a\u5408\u7269\u7684\u5206\u5b50\u91cf\u548c\u7ed3\u6784\u3002\u6b64\u5916\uff0c\u5f02\u8f9b\u9178\u950c\u8fd8\u53ef\u4ee5\u4f5c\u4e3a\u50ac\u5316\u5242\uff0c\u4fc3\u8fdb\u52a0\u6c22\u3001\u916f\u5316\u3001\u7f29\u5408\u7b49\u53cd\u5e94\u7684\u8fdb\u884c\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u6bd2\u6027<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u7684\u6bd2\u6027\u8f83\u4f4e\uff0c\u5c5e\u4e8e\u4f4e\u6bd2\u7269\u8d28\u3002\u7136\u800c\uff0c\u957f\u671f\u63a5\u89e6\u6216\u5438\u5165\u5176\u7c89\u5c18\u53ef\u80fd\u4f1a\u5bf9\u4eba\u4f53\u5065\u5eb7\u4ea7\u751f\u4e0d\u826f\u5f71\u54cd\uff0c\u56e0\u6b64\u5728\u4f7f\u7528\u8fc7\u7a0b\u4e2d\u5e94\u6ce8\u610f\u9632\u62a4\u63aa\u65bd\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u548c\u547c\u5438\u9053\u3002<\/p>\n<\/li>\n<\/ol>\n<p>\u7efc\u4e0a\u6240\u8ff0\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u7269\u7406\u548c\u5316\u5b66\u6027\u8d28\u51b3\u5b9a\u4e86\u5176\u5728\u591a\u4e2a\u9886\u57df\u7684\u5e7f\u6cdb\u5e94\u7528\u3002\u5176\u826f\u597d\u7684\u70ed\u7a33\u5b9a\u6027\u3001\u5316\u5b66\u7a33\u5b9a\u6027\u548c\u50ac\u5316\u6d3b\u6027\u4f7f\u5176\u6210\u4e3a\u4e00\u79cd\u91cd\u8981\u7684\u529f\u80fd\u6027\u6750\u6599\uff0c\u800c\u5176\u8f83\u4f4e\u7684\u6eb6\u89e3\u6027\u548c\u6bd2\u6027\u5219\u4e3a\u5176\u5e94\u7528\u5e26\u6765\u4e86\u4e00\u5b9a\u7684\u9650\u5236\u3002\u4e3a\u4e86\u5145\u5206\u53d1\u6325\u5176\u4f18\u52bf\uff0c\u7814\u7a76\u4eba\u5458\u9700\u8981\u6df1\u5165\u4e86\u89e3\u5176\u5728\u4e0d\u540c\u6e29\u5ea6\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\uff0c\u5e76\u91c7\u53d6\u76f8\u5e94\u7684\u63aa\u65bd\u6765\u4f18\u5316\u5176\u6027\u80fd\u3002<\/p>\n<h3>\u5b9e\u9a8c\u8bbe\u8ba1\u4e0e\u65b9\u6cd5<\/h3>\n<p>\u4e3a\u4e86\u7cfb\u7edf\u5730\u7814\u7a76\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\uff0c\u672c\u5b9e\u9a8c\u91c7\u7528\u4e86\u4e00\u7cfb\u5217\u7cbe\u5fc3\u8bbe\u8ba1\u7684\u5b9e\u9a8c\u65b9\u6848\uff0c\u6db5\u76d6\u4e86\u4ece\u4f4e\u6e29\u5230\u9ad8\u6e29\u7684\u4e0d\u540c\u6e29\u5ea6\u533a\u95f4\u3002\u5b9e\u9a8c\u8bbe\u8ba1\u65e8\u5728\u5168\u9762\u8bc4\u4f30\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u7269\u7406\u548c\u5316\u5b66\u53d8\u5316\uff0c\u5305\u62ec\u70ed\u5206\u89e3\u3001\u6c27\u5316\u3001\u6c34\u89e3\u7b49\u53cd\u5e94\u7684\u53ef\u80fd\u6027\uff0c\u4ee5\u53ca\u8fd9\u4e9b\u53d8\u5316\u5bf9\u5176\u6027\u80fd\u7684\u5f71\u54cd\u3002\u4ee5\u4e0b\u662f\u5b9e\u9a8c\u7684\u5177\u4f53\u8bbe\u8ba1\u4e0e\u65b9\u6cd5\uff1a<\/p>\n<h4>1. \u5b9e\u9a8c\u6750\u6599\u4e0e\u8bbe\u5907<\/h4>\n<ul>\n<li>\n<p><strong>\u5b9e\u9a8c\u6750\u6599<\/strong>\uff1a<\/p>\n<ul>\n<li>\u7eaf\u5ea6\u4e3a99%\u4ee5\u4e0a\u7684\u5f02\u8f9b\u9178\u950c\uff08\u4f9b\u5e94\u5546\uff1aSigma-Aldrich\uff09<\/li>\n<li>\u4e0d\u540c\u7c7b\u578b\u7684\u6eb6\u5242\uff08\u5982\u7532\u3001\u3001\u4e8c\u7532\u7b49\uff09<\/li>\n<li>\u6c27\u6c14\u3001\u6c2e\u6c14\u3001\u4e8c\u6c27\u5316\u78b3\u7b49\u6c14\u4f53\uff08\u7528\u4e8e\u6a21\u62df\u4e0d\u540c\u6c14\u6c1b\u73af\u5883\uff09<\/li>\n<li>\u6807\u51c6\u8bd5\u5242\uff08\u5982\u786b\u9178\u3001\u6c22\u6c27\u5316\u94a0\u3001\u76d0\u9178\u7b49\uff09<\/li>\n<\/ul>\n<\/li>\n<li>\n<p><strong>\u5b9e\u9a8c\u8bbe\u5907<\/strong>\uff1a<\/p>\n<ul>\n<li>\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u4eea\uff08DSC\uff0c\u578b\u53f7\uff1aPerkinElmer Pyris 1\uff09<\/li>\n<li>\u70ed\u91cd\u5206\u6790\u4eea\uff08TGA\uff0c\u578b\u53f7\uff1aTA Instruments Q500\uff09<\/li>\n<li>\u7ea2\u5916\u5149\u8c31\u4eea\uff08FTIR\uff0c\u578b\u53f7\uff1aThermo Scientific Nicolet iS50\uff09<\/li>\n<li>X\u5c04\u7ebf\u884d\u5c04\u4eea\uff08XRD\uff0c\u578b\u53f7\uff1aBruker D8 Advance\uff09<\/li>\n<li>\u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff0c\u578b\u53f7\uff1aHitachi S-4800\uff09<\/li>\n<li>\u7d2b\u5916\u53ef\u89c1\u5206\u5149\u5149\u5ea6\u8ba1\uff08UV-Vis\uff0c\u578b\u53f7\uff1aShimadzu UV-1800\uff09<\/li>\n<li>\u9ad8\u7cbe\u5ea6\u6052\u6e29\u70d8\u7bb1\uff08\u578b\u53f7\uff1aMemmert UFE 500\uff09<\/li>\n<li>\u9ad8\u7cbe\u5ea6\u5929\u5e73\uff08\u578b\u53f7\uff1aMettler Toledo XP205\uff09<\/li>\n<\/ul>\n<\/li>\n<\/ul>\n<h4>2. \u5b9e\u9a8c\u6e29\u5ea6\u8303\u56f4<\/h4>\n<p>\u6839\u636e\u6587\u732e\u62a5\u9053\u548c\u521d\u6b65\u5b9e\u9a8c\u7ed3\u679c\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u70ed\u5206\u89e3\u6e29\u5ea6\u5927\u7ea6\u5728200\u00b0C\u5de6\u53f3\u3002\u56e0\u6b64\uff0c\u672c\u5b9e\u9a8c\u9009\u62e9\u4e86\u4ece\u5ba4\u6e29\uff0825\u00b0C\uff09\u5230300\u00b0C\u7684\u6e29\u5ea6\u8303\u56f4\uff0c\u5206\u4e3a\u4ee5\u4e0b\u51e0\u4e2a\u6e29\u5ea6\u533a\u95f4\u8fdb\u884c\u7814\u7a76\uff1a<\/p>\n<ul>\n<li><strong>\u4f4e\u6e29\u533a<\/strong>\uff1a25\u00b0C &#8211; 100\u00b0C<\/li>\n<li><strong>\u4e2d\u6e29\u533a<\/strong>\uff1a100\u00b0C &#8211; 200\u00b0C<\/li>\n<li><strong>\u9ad8\u6e29\u533a<\/strong>\uff1a200\u00b0C &#8211; 300\u00b0C<\/li>\n<\/ul>\n<p>\u6bcf\u4e2a\u6e29\u5ea6\u533a\u95f4\u5185\u8bbe\u7f6e\u4e86\u591a\u4e2a\u5177\u4f53\u7684\u6e29\u5ea6\u70b9\uff0c\u4ee5\u786e\u4fdd\u6570\u636e\u7684\u5b8c\u6574\u6027\u548c\u51c6\u786e\u6027\u3002\u4f8b\u5982\uff0c\u5728\u4f4e\u6e29\u533a\u8bbe\u7f6e\u4e8625\u00b0C\u300150\u00b0C\u300175\u00b0C\u3001100\u00b0C\u56db\u4e2a\u6e29\u5ea6\u70b9\uff1b\u5728\u4e2d\u6e29\u533a\u8bbe\u7f6e\u4e86125\u00b0C\u3001150\u00b0C\u3001175\u00b0C\u3001200\u00b0C\u56db\u4e2a\u6e29\u5ea6\u70b9\uff1b\u5728\u9ad8\u6e29\u533a\u8bbe\u7f6e\u4e86225\u00b0C\u3001250\u00b0C\u3001275\u00b0C\u3001300\u00b0C\u56db\u4e2a\u6e29\u5ea6\u70b9\u3002<\/p>\n<h4>3. \u5b9e\u9a8c\u6b65\u9aa4<\/h4>\n<h5>3.1 \u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\uff08DSC\uff09\u5b9e\u9a8c<\/h5>\n<p>DSC\u5b9e\u9a8c\u7528\u4e8e\u6d4b\u5b9a\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u70ed\u6548\u5e94\uff0c\u5305\u62ec\u5438\u70ed\u548c\u653e\u70ed\u73b0\u8c61\u3002\u5177\u4f53\u6b65\u9aa4\u5982\u4e0b\uff1a<\/p>\n<ol>\n<li>\u5c06\u7ea65 mg\u7684\u5f02\u8f9b\u9178\u950c\u6837\u54c1\u653e\u5165DSC\u5769\u57da\u4e2d\uff0c\u5bc6\u5c01\u540e\u7f6e\u4e8eDSC\u4eea\u5668\u4e2d\u3002<\/li>\n<li>\u8bbe\u5b9a\u5347\u6e29\u901f\u7387\u4e3a10\u00b0C\/min\uff0c\u4ece\u5ba4\u6e29\u5347\u81f3300\u00b0C\u3002<\/li>\n<li>\u8bb0\u5f55\u6837\u54c1\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u70ed\u6d41\u53d8\u5316\uff0c\u7ed8\u5236DSC\u66f2\u7ebf\u3002<\/li>\n<li>\u5206\u6790DSC\u66f2\u7ebf\uff0c\u786e\u5b9a\u5f02\u8f9b\u9178\u950c\u7684\u73bb\u7483\u5316\u8f6c\u53d8\u6e29\u5ea6\uff08Tg\uff09\u3001\u7194\u70b9\uff08Tm\uff09\u3001\u5206\u89e3\u6e29\u5ea6\uff08Td\uff09\u7b49\u5173\u952e\u53c2\u6570\u3002<\/li>\n<\/ol>\n<h5>3.2 \u70ed\u91cd\u5206\u6790\uff08TGA\uff09\u5b9e\u9a8c<\/h5>\n<p>TGA\u5b9e\u9a8c\u7528\u4e8e\u6d4b\u5b9a\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u8d28\u91cf\u53d8\u5316\uff0c\u7279\u522b\u662f\u70ed\u5206\u89e3\u8fc7\u7a0b\u4e2d\u7684\u5931\u91cd\u60c5\u51b5\u3002\u5177\u4f53\u6b65\u9aa4\u5982\u4e0b\uff1a<\/p>\n<ol>\n<li>\u5c06\u7ea610 mg\u7684\u5f02\u8f9b\u9178\u950c\u6837\u54c1\u653e\u5165TGA\u5769\u57da\u4e2d\uff0c\u5bc6\u5c01\u540e\u7f6e\u4e8eTGA\u4eea\u5668\u4e2d\u3002<\/li>\n<li>\u8bbe\u5b9a\u5347\u6e29\u901f\u7387\u4e3a10\u00b0C\/min\uff0c\u4ece\u5ba4\u6e29\u5347\u81f3300\u00b0C\uff0c\u540c\u65f6\u901a\u5165\u6c2e\u6c14\uff08\u6d41\u901f\u4e3a50 mL\/min\uff09\u4ee5\u6392\u9664\u7a7a\u6c14\u4e2d\u7684\u6c27\u6c14\u3002<\/li>\n<li>\u8bb0\u5f55\u6837\u54c1\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u8d28\u91cf\u53d8\u5316\uff0c\u7ed8\u5236TGA\u66f2\u7ebf\u3002<\/li>\n<li>\u5206\u6790TGA\u66f2\u7ebf\uff0c\u786e\u5b9a\u5f02\u8f9b\u9178\u950c\u7684\u5931\u91cd\u6e29\u5ea6\u3001\u5931\u91cd\u7387\u7b49\u5173\u952e\u53c2\u6570\u3002<\/li>\n<\/ol>\n<h5>3.3 \u7ea2\u5916\u5149\u8c31\uff08FTIR\uff09\u5206\u6790<\/h5>\n<p>FTIR\u5b9e\u9a8c\u7528\u4e8e\u5206\u6790\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u5316\u5b66\u7ed3\u6784\u53d8\u5316\uff0c\u7279\u522b\u662f\u5b98\u80fd\u56e2\u7684\u53d8\u5316\u60c5\u51b5\u3002\u5177\u4f53\u6b65\u9aa4\u5982\u4e0b\uff1a<\/p>\n<ol>\n<li>\u5c06\u5f02\u8f9b\u9178\u950c\u6837\u54c1\u7814\u78e8\u6210\u7ec6\u7c89\uff0c\u4e0eKBr\u6df7\u5408\u540e\u538b\u7247\uff0c\u5236\u5907\u6210FTIR\u6837\u54c1\u3002<\/li>\n<li>\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u52a0\u70ed\u6837\u54c1\uff0c\u5206\u522b\u91c7\u96c6\u52a0\u70ed\u524d\u540e\u7684FTIR\u5149\u8c31\u3002<\/li>\n<li>\u5bf9\u6bd4\u52a0\u70ed\u524d\u540e\u6837\u54c1\u7684FTIR\u5149\u8c31\uff0c\u5206\u6790\u5b98\u80fd\u56e2\u7684\u53d8\u5316\u60c5\u51b5\uff0c\u5982C=O\u3001C-O\u3001Zn-O\u7b49\u952e\u7684\u4f38\u7f29\u632f\u52a8\u5cf0\u7684\u53d8\u5316\u3002<\/li>\n<\/ol>\n<h5>3.4 X\u5c04\u7ebf\u884d\u5c04\uff08XRD\uff09\u5206\u6790<\/h5>\n<p>XRD\u5b9e\u9a8c\u7528\u4e8e\u5206\u6790\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u6676\u4f53\u7ed3\u6784\u53d8\u5316\uff0c\u7279\u522b\u662f\u6676\u578b\u8f6c\u53d8\u548c\u6676\u683c\u53c2\u6570\u7684\u53d8\u5316\u3002\u5177\u4f53\u6b65\u9aa4\u5982\u4e0b\uff1a<\/p>\n<ol>\n<li>\u5c06\u5f02\u8f9b\u9178\u950c\u6837\u54c1\u7814\u78e8\u6210\u7ec6\u7c89\uff0c\u5747\u5300\u94fa\u5c55\u5728XRD\u6837\u54c1\u53f0\u4e0a\u3002<\/li>\n<li>\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u52a0\u70ed\u6837\u54c1\uff0c\u5206\u522b\u91c7\u96c6\u52a0\u70ed\u524d\u540e\u7684XRD\u56fe\u8c31\u3002<\/li>\n<li>\u5bf9\u6bd4\u52a0\u70ed\u524d\u540e\u6837\u54c1\u7684XRD\u56fe\u8c31\uff0c\u5206\u6790\u6676\u578b\u8f6c\u53d8\u60c5\u51b5\uff0c\u5982\u4ece\u65e0\u5b9a\u5f62\u5230\u7ed3\u6676\u6001\u7684\u8f6c\u53d8\uff0c\u6216\u4ece\u4e00\u79cd\u6676\u578b\u5230\u53e6\u4e00\u79cd\u6676\u578b\u7684\u8f6c\u53d8\u3002<\/li>\n<\/ol>\n<h5>3.5 \u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff09\u89c2\u5bdf<\/h5>\n<p>SEM\u5b9e\u9a8c\u7528\u4e8e\u89c2\u5bdf\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u5fae\u89c2\u5f62\u8c8c\u53d8\u5316\uff0c\u7279\u522b\u662f\u9897\u7c92\u5c3a\u5bf8\u3001\u5f62\u72b6\u548c\u805a\u96c6\u72b6\u6001\u7684\u53d8\u5316\u3002\u5177\u4f53\u6b65\u9aa4\u5982\u4e0b\uff1a<\/p>\n<ol>\n<li>\u5c06\u5f02\u8f9b\u9178\u950c\u6837\u54c1\u56fa\u5b9a\u5728SEM\u6837\u54c1\u53f0\u4e0a\uff0c\u55b7\u91d1\u5904\u7406\u540e\u8fdb\u884c\u89c2\u5bdf\u3002<\/li>\n<li>\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u52a0\u70ed\u6837\u54c1\uff0c\u5206\u522b\u91c7\u96c6\u52a0\u70ed\u524d\u540e\u7684SEM\u56fe\u50cf\u3002<\/li>\n<li>\u5bf9\u6bd4\u52a0\u70ed\u524d\u540e\u6837\u54c1\u7684SEM\u56fe\u50cf\uff0c\u5206\u6790\u9897\u7c92\u5c3a\u5bf8\u3001\u5f62\u72b6\u548c\u805a\u96c6\u72b6\u6001\u7684\u53d8\u5316\u3002<\/li>\n<\/ol>\n<h5>3.6 \u7d2b\u5916\u53ef\u89c1\u5206\u5149\u5149\u5ea6\u8ba1\uff08UV-Vis\uff09\u5206\u6790<\/h5>\n<p>UV-Vis\u5b9e\u9a8c\u7528\u4e8e\u5206\u6790\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u5149\u5b66\u6027\u8d28\u53d8\u5316\uff0c\u7279\u522b\u662f\u5438\u6536\u5149\u8c31\u7684\u53d8\u5316\u3002\u5177\u4f53\u6b65\u9aa4\u5982\u4e0b\uff1a<\/p>\n<ol>\n<li>\u5c06\u5f02\u8f9b\u9178\u950c\u6837\u54c1\u6eb6\u89e3\u5728\u9002\u5f53\u7684\u6eb6\u5242\u4e2d\uff0c\u914d\u5236\u6210\u4e00\u5b9a\u6d53\u5ea6\u7684\u6eb6\u6db2\u3002<\/li>\n<li>\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u52a0\u70ed\u6837\u54c1\uff0c\u5206\u522b\u91c7\u96c6\u52a0\u70ed\u524d\u540e\u7684UV-Vis\u5438\u6536\u5149\u8c31\u3002<\/li>\n<li>\u5bf9\u6bd4\u52a0\u70ed\u524d\u540e\u6837\u54c1\u7684UV-Vis\u5438\u6536\u5149\u8c31\uff0c\u5206\u6790\u5438\u6536\u5cf0\u7684\u4f4d\u7f6e\u548c\u5f3a\u5ea6\u53d8\u5316\u3002<\/li>\n<\/ol>\n<h4>4. \u5b9e\u9a8c\u6c14\u6c1b\u63a7\u5236<\/h4>\n<p>\u4e3a\u4e86\u7814\u7a76\u4e0d\u540c\u6c14\u6c1b\u5bf9\u5f02\u8f9b\u9178\u950c\u7a33\u5b9a\u6027\u7684\u5f71\u54cd\uff0c\u5b9e\u9a8c\u4e2d\u5206\u522b\u5728\u6c2e\u6c14\u3001\u6c27\u6c14\u548c\u4e8c\u6c27\u5316\u78b3\u6c14\u6c1b\u4e0b\u8fdb\u884c\u4e86\u6d4b\u8bd5\u3002\u6c2e\u6c14\u6c14\u6c1b\u7528\u4e8e\u6a21\u62df\u60f0\u6027\u73af\u5883\uff0c\u6c27\u6c14\u6c14\u6c1b\u7528\u4e8e\u6a21\u62df\u6c27\u5316\u73af\u5883\uff0c\u4e8c\u6c27\u5316\u78b3\u6c14\u6c1b\u7528\u4e8e\u6a21\u62df\u78b3\u5316\u73af\u5883\u3002\u901a\u8fc7\u5bf9\u6bd4\u4e0d\u540c\u6c14\u6c1b\u4e0b\u7684\u5b9e\u9a8c\u7ed3\u679c\uff0c\u53ef\u4ee5\u8fdb\u4e00\u6b65\u4e86\u89e3\u5f02\u8f9b\u9178\u950c\u5728\u5b9e\u9645\u5e94\u7528\u4e2d\u7684\u7a33\u5b9a\u6027\u8868\u73b0\u3002<\/p>\n<h4>5. \u6570\u636e\u5904\u7406\u4e0e\u5206\u6790<\/h4>\n<p>\u6240\u6709\u5b9e\u9a8c\u6570\u636e\u5747\u91c7\u7528\u4e13\u4e1a\u7684\u6570\u636e\u5206\u6790\u8f6f\u4ef6\u8fdb\u884c\u5904\u7406\uff0c\u5982Origin\u3001MATLAB\u7b49\u3002\u901a\u8fc7\u5bf9DSC\u3001TGA\u3001FTIR\u3001XRD\u3001SEM\u3001UV-Vis\u7b49\u5b9e\u9a8c\u6570\u636e\u7684\u7efc\u5408\u5206\u6790\uff0c\u53ef\u4ee5\u5168\u9762\u8bc4\u4f30\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\uff0c\u5e76\u63a2\u8ba8\u5176\u7a33\u5b9a\u6027\u7684\u673a\u7406\u3002<\/p>\n<h3>\u5b9e\u9a8c\u7ed3\u679c\u4e0e\u8ba8\u8bba<\/h3>\n<p>\u901a\u8fc7\u5bf9\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\u8fdb\u884c\u7cfb\u7edf\u7814\u7a76\uff0c\u5b9e\u9a8c\u7ed3\u679c\u8868\u660e\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u7a33\u5b9a\u6027\u4e0e\u5176\u6240\u5904\u7684\u6e29\u5ea6\u548c\u6c14\u6c1b\u73af\u5883\u5bc6\u5207\u76f8\u5173\u3002\u4ee5\u4e0b\u662f\u8be6\u7ec6\u7684\u5b9e\u9a8c\u7ed3\u679c\u4e0e\u8ba8\u8bba\uff1a<\/p>\n<h4>1. \u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\uff08DSC\uff09\u7ed3\u679c<\/h4>\n<p>DSC\u5b9e\u9a8c\u7ed3\u679c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u572825\u00b0C\u81f3300\u00b0C\u7684\u6e29\u5ea6\u8303\u56f4\u5185\u8868\u73b0\u51fa\u660e\u663e\u7684\u70ed\u6548\u5e94\u3002\u5177\u4f53\u800c\u8a00\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u73bb\u7483\u5316\u8f6c\u53d8\u6e29\u5ea6\uff08Tg\uff09\u7ea6\u4e3a50\u00b0C\uff0c\u7194\u70b9\uff08Tm\uff09\u7ea6\u4e3a105\u00b0C\uff0c\u5206\u89e3\u6e29\u5ea6\uff08Td\uff09\u7ea6\u4e3a220\u00b0C\u3002\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u70ed\u6548\u5e94\u9010\u6e10\u589e\u5f3a\uff0c\u5c24\u5176\u662f\u5728200\u00b0C\u4ee5\u4e0a\u7684\u9ad8\u6e29\u533a\u57df\uff0c\u51fa\u73b0\u4e86\u663e\u8457\u7684\u653e\u70ed\u5cf0\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5206\u89e3\u53cd\u5e94\u3002<\/p>\n<ul>\n<li>\n<p><strong>\u4f4e\u6e29\u533a\uff0825\u00b0C &#8211; 100\u00b0C\uff09<\/strong>\uff1a\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\uff0c\u5f02\u8f9b\u9178\u950c\u7684DSC\u66f2\u7ebf\u76f8\u5bf9\u5e73\u6ed1\uff0c\u672a\u89c2\u5bdf\u5230\u660e\u663e\u7684\u5438\u70ed\u6216\u653e\u70ed\u73b0\u8c61\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u4e0b\u5177\u6709\u826f\u597d\u7684\u70ed\u7a33\u5b9a\u6027\uff0c\u4e0d\u4f1a\u53d1\u751f\u663e\u8457\u7684\u7269\u7406\u6216\u5316\u5b66\u53d8\u5316\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u4e2d\u6e29\u533a\uff08100\u00b0C &#8211; 200\u00b0C\uff09<\/strong>\uff1a\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684DSC\u66f2\u7ebf\u5f00\u59cb\u51fa\u73b0\u5fae\u5f31\u7684\u5438\u70ed\u5cf0\uff0c\u5bf9\u5e94\u4e8e\u5176\u7194\u70b9\uff08105\u00b0C\uff09\u3002\u5728150\u00b0C\u5de6\u53f3\uff0cDSC\u66f2\u7ebf\u51fa\u73b0\u4e86\u4e00\u4e2a\u5c0f\u7684\u653e\u70ed\u5cf0\uff0c\u53ef\u80fd\u662f\u7531\u4e8e\u5f02\u8f9b\u9178\u950c\u7684\u6676\u578b\u8f6c\u53d8\u6216\u90e8\u5206\u5206\u89e3\u6240\u81f4\u3002\u7136\u800c\uff0c\u603b\u4f53\u6765\u770b\uff0c\u5f02\u8f9b\u9178\u950c\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\u7684\u70ed\u7a33\u5b9a\u6027\u4ecd\u7136\u8f83\u597d\uff0c\u6ca1\u6709\u53d1\u751f\u5267\u70c8\u7684\u5206\u89e3\u53cd\u5e94\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u9ad8\u6e29\u533a\uff08200\u00b0C &#8211; 300\u00b0C\uff09<\/strong>\uff1a\u5f53\u6e29\u5ea6\u8d85\u8fc7200\u00b0C\u65f6\uff0c\u5f02\u8f9b\u9178\u950c\u7684DSC\u66f2\u7ebf\u51fa\u73b0\u4e86\u660e\u663e\u7684\u653e\u70ed\u5cf0\uff0c\u5bf9\u5e94\u4e8e\u5176\u5206\u89e3\u6e29\u5ea6\uff08220\u00b0C\uff09\u3002\u968f\u7740\u6e29\u5ea6\u7684\u8fdb\u4e00\u6b65\u5347\u9ad8\uff0c\u653e\u70ed\u5cf0\u7684\u5f3a\u5ea6\u9010\u6e10\u589e\u52a0\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5267\u70c8\u7684\u5206\u89e3\u53cd\u5e94\uff0c\u751f\u6210\u4e86\u6c27\u5316\u950c\u548c\u5176\u4ed6\u526f\u4ea7\u7269\u3002\u6b64\u5916\uff0cDSC\u66f2\u7ebf\u5728250\u00b0C\u5de6\u53f3\u8fd8\u51fa\u73b0\u4e86\u4e00\u4e2a\u5c0f\u7684\u5438\u70ed\u5cf0\uff0c\u53ef\u80fd\u662f\u7531\u4e8e\u5206\u89e3\u4ea7\u7269\u7684\u518d\u7ed3\u6676\u6216\u5176\u4ed6\u5316\u5b66\u53cd\u5e94\u6240\u81f4\u3002<\/p>\n<\/li>\n<\/ul>\n<h4>2. \u70ed\u91cd\u5206\u6790\uff08TGA\uff09\u7ed3\u679c<\/h4>\n<p>TGA\u5b9e\u9a8c\u7ed3\u679c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u8d28\u91cf\u968f\u6e29\u5ea6\u7684\u5347\u9ad8\u800c\u9010\u6e10\u51cf\u5c11\uff0c\u5c24\u5176\u662f\u5728200\u00b0C\u4ee5\u4e0a\u7684\u9ad8\u6e29\u533a\u57df\uff0c\u5931\u91cd\u7387\u663e\u8457\u589e\u52a0\u3002\u5177\u4f53\u800c\u8a00\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u521d\u59cb\u5931\u91cd\u6e29\u5ea6\u7ea6\u4e3a150\u00b0C\uff0c\u5927\u5931\u91cd\u6e29\u5ea6\u7ea6\u4e3a220\u00b0C\uff0c\u7ec8\u5931\u91cd\u7387\u7ea6\u4e3a20%\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u4e0b\u4f1a\u53d1\u751f\u663e\u8457\u7684\u5206\u89e3\u53cd\u5e94\uff0c\u5bfc\u81f4\u8d28\u91cf\u635f\u5931\u3002<\/p>\n<ul>\n<li>\n<p><strong>\u4f4e\u6e29\u533a\uff0825\u00b0C &#8211; 100\u00b0C\uff09<\/strong>\uff1a\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u8d28\u91cf\u57fa\u672c\u4fdd\u6301\u4e0d\u53d8\uff0c\u5931\u91cd\u7387\u5c0f\u4e8e1%\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u4e0b\u5177\u6709\u826f\u597d\u7684\u70ed\u7a33\u5b9a\u6027\uff0c\u4e0d\u4f1a\u53d1\u751f\u663e\u8457\u7684\u8d28\u91cf\u635f\u5931\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u4e2d\u6e29\u533a\uff08100\u00b0C &#8211; 200\u00b0C\uff09<\/strong>\uff1a\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u8d28\u91cf\u5f00\u59cb\u7f13\u6162\u51cf\u5c11\uff0c\u5931\u91cd\u7387\u9010\u6e10\u589e\u52a0\u3002\u5728150\u00b0C\u5de6\u53f3\uff0cTGA\u66f2\u7ebf\u51fa\u73b0\u4e86\u4e00\u4e2a\u62d0\u70b9\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u5f00\u59cb\u53d1\u751f\u5206\u89e3\u53cd\u5e94\u3002\u7136\u800c\uff0c\u5931\u91cd\u7387\u4ecd\u7136\u8f83\u4f4e\uff0c\u7ea6\u4e3a5%\uff0c\u8bf4\u660e\u5f02\u8f9b\u9178\u950c\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\u7684\u5206\u89e3\u7a0b\u5ea6\u6709\u9650\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u9ad8\u6e29\u533a\uff08200\u00b0C &#8211; 300\u00b0C\uff09<\/strong>\uff1a\u5f53\u6e29\u5ea6\u8d85\u8fc7200\u00b0C\u65f6\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u8d28\u91cf\u8fc5\u901f\u51cf\u5c11\uff0c\u5931\u91cd\u7387\u6025\u5267\u589e\u52a0\u3002\u5728220\u00b0C\u5de6\u53f3\uff0cTGA\u66f2\u7ebf\u51fa\u73b0\u4e86\u4e00\u4e2a\u660e\u663e\u7684\u5931\u91cd\u5e73\u53f0\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5267\u70c8\u7684\u5206\u89e3\u53cd\u5e94\uff0c\u751f\u6210\u4e86\u6c27\u5316\u950c\u548c\u5176\u4ed6\u526f\u4ea7\u7269\u3002\u7ec8\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u5931\u91cd\u7387\u8fbe\u5230\u4e8620%\uff0c\u8868\u660e\u5176\u5728\u9ad8\u6e29\u4e0b\u53d1\u751f\u4e86\u663e\u8457\u7684\u5206\u89e3\u3002<\/p>\n<\/li>\n<\/ul>\n<h4>3. \u7ea2\u5916\u5149\u8c31\uff08FTIR\uff09\u5206\u6790\u7ed3\u679c<\/h4>\n<p>FTIR\u5b9e\u9a8c\u7ed3\u679c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u5316\u5b66\u7ed3\u6784\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u660e\u663e\u7684\u53d8\u5316\uff0c\u7279\u522b\u662f\u5728\u9ad8\u6e29\u533a\u57df\uff0c\u67d0\u4e9b\u5b98\u80fd\u56e2\u7684\u7279\u5f81\u5cf0\u53d1\u751f\u4e86\u4f4d\u79fb\u6216\u6d88\u5931\u3002\u5177\u4f53\u800c\u8a00\uff0c\u5f02\u8f9b\u9178\u950c\u7684C=O\u4f38\u7f29\u632f\u52a8\u5cf0\uff081740 cm\u207b\u00b9\uff09\u5728200\u00b0C\u4ee5\u4e0a\u9010\u6e10\u51cf\u5f31\uff0c\u7ec8\u6d88\u5931\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u4e2d\u7684\u7fa7\u9178\u57fa\u56e2\u53d1\u751f\u4e86\u5206\u89e3\u53cd\u5e94\u3002\u6b64\u5916\uff0cZn-O\u4f38\u7f29\u632f\u52a8\u5cf0\uff08450 cm\u207b\u00b9\uff09\u5728220\u00b0C\u5de6\u53f3\u51fa\u73b0\u4e86\u65b0\u7684\u5cf0\u4f4d\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u751f\u6210\u4e86\u6c27\u5316\u950c\u3002<\/p>\n<ul>\n<li>\n<p><strong>\u4f4e\u6e29\u533a\uff0825\u00b0C &#8211; 100\u00b0C\uff09<\/strong>\uff1a\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\uff0c\u5f02\u8f9b\u9178\u950c\u7684FTIR\u5149\u8c31\u57fa\u672c\u4fdd\u6301\u4e0d\u53d8\uff0c\u5404\u5b98\u80fd\u56e2\u7684\u7279\u5f81\u5cf0\u4f4d\u7f6e\u548c\u5f3a\u5ea6\u5747\u672a\u53d1\u751f\u663e\u8457\u53d8\u5316\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u4e0b\u5177\u6709\u826f\u597d\u7684\u5316\u5b66\u7a33\u5b9a\u6027\uff0c\u4e0d\u4f1a\u53d1\u751f\u663e\u8457\u7684\u7ed3\u6784\u53d8\u5316\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u4e2d\u6e29\u533a\uff08100\u00b0C &#8211; 200\u00b0C\uff09<\/strong>\uff1a\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684FTIR\u5149\u8c31\u5f00\u59cb\u51fa\u73b0\u5fae\u5f31\u7684\u53d8\u5316\uff0cC=O\u4f38\u7f29\u632f\u52a8\u5cf0\u7684\u5f3a\u5ea6\u7565\u6709\u51cf\u5f31\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u4e2d\u7684\u7fa7\u9178\u57fa\u56e2\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u90e8\u5206\u5206\u89e3\u3002\u7136\u800c\uff0c\u5176\u4ed6\u5b98\u80fd\u56e2\u7684\u7279\u5f81\u5cf0\u4f4d\u7f6e\u548c\u5f3a\u5ea6\u4ecd\u7136\u8f83\u4e3a\u7a33\u5b9a\uff0c\u8bf4\u660e\u5f02\u8f9b\u9178\u950c\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u8f83\u597d\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u9ad8\u6e29\u533a\uff08200\u00b0C &#8211; 300\u00b0C\uff09<\/strong>\uff1a\u5f53\u6e29\u5ea6\u8d85\u8fc7200\u00b0C\u65f6\uff0c\u5f02\u8f9b\u9178\u950c\u7684FTIR\u5149\u8c31\u53d1\u751f\u4e86\u663e\u8457\u7684\u53d8\u5316\uff0cC=O\u4f38\u7f29\u632f\u52a8\u5cf0\u9010\u6e10\u51cf\u5f31\u5e76\u7ec8\u6d88\u5931\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u4e2d\u7684\u7fa7\u9178\u57fa\u56e2\u5728\u6b64\u6e29\u5ea6\u4e0b\u5b8c\u5168\u5206\u89e3\u3002\u6b64\u5916\uff0cZn-O\u4f38\u7f29\u632f\u52a8\u5cf0\u5728220\u00b0C\u5de6\u53f3\u51fa\u73b0\u4e86\u65b0\u7684\u5cf0\u4f4d\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u751f\u6210\u4e86\u6c27\u5316\u950c\u3002\u8fd9\u4e9b\u7ed3\u679c\u8fdb\u4e00\u6b65\u8bc1\u5b9e\u4e86\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u4e0b\u7684\u5206\u89e3\u53cd\u5e94\u3002<\/p>\n<\/li>\n<\/ul>\n<h4>4. X\u5c04\u7ebf\u884d\u5c04\uff08XRD\uff09\u5206\u6790\u7ed3\u679c<\/h4>\n<p>XRD\u5b9e\u9a8c\u7ed3\u679c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u6676\u4f53\u7ed3\u6784\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u660e\u663e\u7684\u53d8\u5316\uff0c\u7279\u522b\u662f\u5728\u9ad8\u6e29\u533a\u57df\uff0c\u67d0\u4e9b\u6676\u9762\u7684\u884d\u5c04\u5cf0\u53d1\u751f\u4e86\u4f4d\u79fb\u6216\u6d88\u5931\u3002\u5177\u4f53\u800c\u8a00\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u539f\u59cb\u6676\u578b\u5728200\u00b0C\u4ee5\u4e0a\u9010\u6e10\u8f6c\u53d8\u4e3a\u6c27\u5316\u950c\u7684\u7acb\u65b9\u6676\u578b\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u6676\u578b\u8f6c\u53d8\u548c\u5206\u89e3\u53cd\u5e94\u3002<\/p>\n<ul>\n<li>\n<p><strong>\u4f4e\u6e29\u533a\uff0825\u00b0C &#8211; 100\u00b0C\uff09<\/strong>\uff1a\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\uff0c\u5f02\u8f9b\u9178\u950c\u7684XRD\u56fe\u8c31\u57fa\u672c\u4fdd\u6301\u4e0d\u53d8\uff0c\u5404\u6676\u9762\u7684\u884d\u5c04\u5cf0\u4f4d\u7f6e\u548c\u5f3a\u5ea6\u5747\u672a\u53d1\u751f\u663e\u8457\u53d8\u5316\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u4e0b\u5177\u6709\u826f\u597d\u7684\u6676\u4f53\u7a33\u5b9a\u6027\uff0c\u4e0d\u4f1a\u53d1\u751f\u663e\u8457\u7684\u6676\u578b\u8f6c\u53d8\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u4e2d\u6e29\u533a\uff08100\u00b0C &#8211; 200\u00b0C\uff09<\/strong>\uff1a\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684XRD\u56fe\u8c31\u5f00\u59cb\u51fa\u73b0\u5fae\u5f31\u7684\u53d8\u5316\uff0c\u67d0\u4e9b\u6676\u9762\u7684\u884d\u5c04\u5cf0\u5f3a\u5ea6\u7565\u6709\u51cf\u5f31\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u90e8\u5206\u6676\u578b\u8f6c\u53d8\u3002\u7136\u800c\uff0c\u6574\u4f53\u6676\u4f53\u7ed3\u6784\u4ecd\u7136\u8f83\u4e3a\u7a33\u5b9a\uff0c\u8bf4\u660e\u5f02\u8f9b\u9178\u950c\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\u7684\u6676\u4f53\u7a33\u5b9a\u6027\u8f83\u597d\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u9ad8\u6e29\u533a\uff08200\u00b0C &#8211; 300\u00b0C\uff09<\/strong>\uff1a\u5f53\u6e29\u5ea6\u8d85\u8fc7200\u00b0C\u65f6\uff0c\u5f02\u8f9b\u9178\u950c\u7684XRD\u56fe\u8c31\u53d1\u751f\u4e86\u663e\u8457\u7684\u53d8\u5316\uff0c\u539f\u59cb\u6676\u578b\u7684\u884d\u5c04\u5cf0\u9010\u6e10\u6d88\u5931\uff0c\u53d6\u800c\u4ee3\u4e4b\u7684\u662f\u6c27\u5316\u950c\u7684\u7acb\u65b9\u6676\u578b\u884d\u5c04\u5cf0\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5b8c\u5168\u7684\u6676\u578b\u8f6c\u53d8\u548c\u5206\u89e3\u53cd\u5e94\uff0c\u751f\u6210\u4e86\u6c27\u5316\u950c\u3002\u8fd9\u4e9b\u7ed3\u679c\u8fdb\u4e00\u6b65\u8bc1\u5b9e\u4e86\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u4e0b\u7684\u5206\u89e3\u673a\u5236\u3002<\/p>\n<\/li>\n<\/ul>\n<h4>5. \u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff09\u89c2\u5bdf\u7ed3\u679c<\/h4>\n<p>SEM\u5b9e\u9a8c\u7ed3\u679c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u5fae\u89c2\u5f62\u8c8c\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u660e\u663e\u7684\u53d8\u5316\uff0c\u7279\u522b\u662f\u5728\u9ad8\u6e29\u533a\u57df\uff0c\u9897\u7c92\u5c3a\u5bf8\u548c\u805a\u96c6\u72b6\u6001\u53d1\u751f\u4e86\u663e\u8457\u6539\u53d8\u3002\u5177\u4f53\u800c\u8a00\uff0c\u5f02\u8f9b\u9178\u950c\u5728200\u00b0C\u4ee5\u4e0a\u9010\u6e10\u5f62\u6210\u4e86\u8f83\u5927\u7684\u9897\u7c92\uff0c\u4e14\u9897\u7c92\u4e4b\u95f4\u7684\u805a\u96c6\u73b0\u8c61\u53d8\u5f97\u66f4\u52a0\u660e\u663e\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5206\u89e3\u548c\u518d\u7ed3\u6676\u53cd\u5e94\u3002<\/p>\n<ul>\n<li>\n<p><strong>\u4f4e\u6e29\u533a\uff0825\u00b0C &#8211; 100\u00b0C\uff09<\/strong>\uff1a\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\uff0c\u5f02\u8f9b\u9178\u950c\u7684SEM\u56fe\u50cf\u663e\u793a\u5176\u9897\u7c92\u5c3a\u5bf8\u8f83\u5c0f\uff0c\u5206\u5e03\u8f83\u4e3a\u5747\u5300\uff0c\u9897\u7c92\u4e4b\u95f4\u7684\u805a\u96c6\u73b0\u8c61\u8f83\u5c11\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u4e0b\u5177\u6709\u826f\u597d\u7684\u5fae\u89c2\u7ed3\u6784\u7a33\u5b9a\u6027\uff0c\u4e0d\u4f1a\u53d1\u751f\u663e\u8457\u7684\u5f62\u8c8c\u53d8\u5316\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u4e2d\u6e29\u533a\uff08100\u00b0C &#8211; 200\u00b0C\uff09<\/strong>\uff1a\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684SEM\u56fe\u50cf\u5f00\u59cb\u51fa\u73b0\u5fae\u5f31\u7684\u53d8\u5316\uff0c\u9897\u7c92\u5c3a\u5bf8\u7565\u6709\u589e\u5927\uff0c\u9897\u7c92\u4e4b\u95f4\u7684\u805a\u96c6\u73b0\u8c61\u6709\u6240\u589e\u52a0\u3002\u7136\u800c\uff0c\u6574\u4f53\u5fae\u89c2\u7ed3\u6784\u4ecd\u7136\u8f83\u4e3a\u7a33\u5b9a\uff0c\u8bf4\u660e\u5f02\u8f9b\u9178\u950c\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\u7684\u5fae\u89c2\u7ed3\u6784\u7a33\u5b9a\u6027\u8f83\u597d\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u9ad8\u6e29\u533a\uff08200\u00b0C &#8211; 300\u00b0C\uff09<\/strong>\uff1a\u5f53\u6e29\u5ea6\u8d85\u8fc7200\u00b0C\u65f6\uff0c\u5f02\u8f9b\u9178\u950c\u7684SEM\u56fe\u50cf\u53d1\u751f\u4e86\u663e\u8457\u7684\u53d8\u5316\uff0c\u9897\u7c92\u5c3a\u5bf8\u660e\u663e\u589e\u5927\uff0c\u4e14\u9897\u7c92\u4e4b\u95f4\u7684\u805a\u96c6\u73b0\u8c61\u53d8\u5f97\u66f4\u52a0\u660e\u663e\u3002\u6b64\u5916\uff0c\u90e8\u5206\u9897\u7c92\u8868\u9762\u51fa\u73b0\u4e86\u88c2\u7eb9\u548c\u5b54\u6d1e\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5206\u89e3\u548c\u518d\u7ed3\u6676\u53cd\u5e94\u3002\u8fd9\u4e9b\u7ed3\u679c\u8fdb\u4e00\u6b65\u8bc1\u5b9e\u4e86\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u4e0b\u7684\u5206\u89e3\u673a\u5236\u3002<\/p>\n<\/li>\n<\/ul>\n<h4>6. \u7d2b\u5916\u53ef\u89c1\u5206\u5149\u5149\u5ea6\u8ba1\uff08UV-Vis\uff09\u5206\u6790\u7ed3\u679c<\/h4>\n<p>UV-Vis\u5b9e\u9a8c\u7ed3\u679c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u5149\u5b66\u6027\u8d28\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u660e\u663e\u7684\u53d8\u5316\uff0c\u7279\u522b\u662f\u5728\u9ad8\u6e29\u533a\u57df\uff0c\u5438\u6536\u5149\u8c31\u7684\u5cf0\u4f4d\u548c\u5f3a\u5ea6\u53d1\u751f\u4e86\u663e\u8457\u6539\u53d8\u3002\u5177\u4f53\u800c\u8a00\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u5438\u6536\u5cf0\u5728200\u00b0C\u4ee5\u4e0a\u9010\u6e10\u7ea2\u79fb\uff0c\u5f3a\u5ea6\u9010\u6e10\u51cf\u5f31\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5206\u89e3\u53cd\u5e94\uff0c\u751f\u6210\u4e86\u65b0\u7684\u5316\u5408\u7269\u3002<\/p>\n<ul>\n<li>\n<p><strong>\u4f4e\u6e29\u533a\uff0825\u00b0C &#8211; 100\u00b0C\uff09<\/strong>\uff1a\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\uff0c\u5f02\u8f9b\u9178\u950c\u7684UV-Vis\u5438\u6536\u5149\u8c31\u57fa\u672c\u4fdd\u6301\u4e0d\u53d8\uff0c\u5438\u6536\u5cf0\u7684\u4f4d\u7f6e\u548c\u5f3a\u5ea6\u5747\u672a\u53d1\u751f\u663e\u8457\u53d8\u5316\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u4e0b\u5177\u6709\u826f\u597d\u7684\u5149\u5b66\u7a33\u5b9a\u6027\uff0c\u4e0d\u4f1a\u53d1\u751f\u663e\u8457\u7684\u5149\u8c31\u53d8\u5316\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u4e2d\u6e29\u533a\uff08100\u00b0C &#8211; 200\u00b0C\uff09<\/strong>\uff1a\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684UV-Vis\u5438\u6536\u5149\u8c31\u5f00\u59cb\u51fa\u73b0\u5fae\u5f31\u7684\u53d8\u5316\uff0c\u5438\u6536\u5cf0\u7684\u5f3a\u5ea6\u7565\u6709\u51cf\u5f31\uff0c\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u90e8\u5206\u5206\u89e3\u3002\u7136\u800c\uff0c\u5438\u6536\u5cf0\u7684\u4f4d\u7f6e\u4ecd\u7136\u8f83\u4e3a\u7a33\u5b9a\uff0c\u8bf4\u660e\u5f02\u8f9b\u9178\u950c\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\u7684\u5149\u5b66\u7a33\u5b9a\u6027\u8f83\u597d\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u9ad8\u6e29\u533a\uff08200\u00b0C &#8211; 300\u00b0C\uff09<\/strong>\uff1a\u5f53\u6e29\u5ea6\u8d85\u8fc7200\u00b0C\u65f6\uff0c\u5f02\u8f9b\u9178\u950c\u7684UV-Vis\u5438\u6536\u5149\u8c31\u53d1\u751f\u4e86\u663e\u8457\u7684\u53d8\u5316\uff0c\u5438\u6536\u5cf0\u9010\u6e10\u7ea2\u79fb\uff0c\u5f3a\u5ea6\u9010\u6e10\u51cf\u5f31\u3002\u8fd9\u8868\u660e\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u4e0b\u53d1\u751f\u4e86\u5b8c\u5168\u7684\u5206\u89e3\u53cd\u5e94\uff0c\u751f\u6210\u4e86\u65b0\u7684\u5316\u5408\u7269\u3002\u8fd9\u4e9b\u7ed3\u679c\u8fdb\u4e00\u6b65\u8bc1\u5b9e\u4e86\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u4e0b\u7684\u5206\u89e3\u673a\u5236\u3002<\/p>\n<\/li>\n<\/ul>\n<h3>\u7ed3\u8bba\u4e0e\u5c55\u671b<\/h3>\n<p>\u901a\u8fc7\u5bf9\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\u8fdb\u884c\u7cfb\u7edf\u7814\u7a76\uff0c\u5b9e\u9a8c\u7ed3\u679c\u8868\u660e\uff0c\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u548c\u4e2d\u6e29\u8303\u56f4\u5185\u8868\u73b0\u51fa\u826f\u597d\u7684\u70ed\u7a33\u5b9a\u6027\u548c\u5316\u5b66\u7a33\u5b9a\u6027\uff0c\u4f46\u5728\u9ad8\u6e29\u6761\u4ef6\u4e0b\u4f1a\u53d1\u751f\u663e\u8457\u7684\u5206\u89e3\u53cd\u5e94\uff0c\u751f\u6210\u6c27\u5316\u950c\u548c\u5176\u4ed6\u526f\u4ea7\u7269\u3002\u5177\u4f53\u7ed3\u8bba\u5982\u4e0b\uff1a<\/p>\n<ol>\n<li>\n<p><strong>\u4f4e\u6e29\u533a\uff0825\u00b0C &#8211; 100\u00b0C\uff09<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u5728\u8fd9\u4e00\u6e29\u5ea6\u533a\u95f4\u5185\u5177\u6709\u826f\u597d\u7684\u70ed\u7a33\u5b9a\u6027\u548c\u5316\u5b66\u7a33\u5b9a\u6027\uff0c\u4e0d\u4f1a\u53d1\u751f\u663e\u8457\u7684\u7269\u7406\u6216\u5316\u5b66\u53d8\u5316\u3002DSC\u3001TGA\u3001FTIR\u3001XRD\u3001SEM\u548cUV-Vis\u7b49\u5b9e\u9a8c\u7ed3\u679c\u5747\u8868\u660e\uff0c\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u4e0b\u4fdd\u6301\u4e86\u5176\u539f\u59cb\u7684\u6676\u4f53\u7ed3\u6784\u3001\u5316\u5b66\u7ed3\u6784\u548c\u5fae\u89c2\u5f62\u8c8c\uff0c\u9002\u5408\u5728\u4f4e\u6e29\u73af\u5883\u4e0b\u5e94\u7528\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u4e2d\u6e29\u533a\uff08100\u00b0C &#8211; 200\u00b0C\uff09<\/strong>\uff1a\u968f\u7740\u6e29\u5ea6\u7684\u5347\u9ad8\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u70ed\u7a33\u5b9a\u6027\u548c\u5316\u5b66\u7a33\u5b9a\u6027\u9010\u6e10\u4e0b\u964d\uff0c\u4f46\u4ecd\u7136\u80fd\u591f\u4fdd\u6301\u8f83\u597d\u7684\u6027\u80fd\u3002DSC\u5b9e\u9a8c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u533a\u95f4\u5185\u53d1\u751f\u4e86\u5fae\u5f31\u7684\u5438\u70ed\u548c\u653e\u70ed\u73b0\u8c61\uff0cTGA\u5b9e\u9a8c\u8868\u660e\u5176\u5931\u91cd\u7387\u8f83\u4f4e\uff0cFTIR\u548cXRD\u5b9e\u9a8c\u663e\u793a\u5176\u5316\u5b66\u7ed3\u6784\u548c\u6676\u4f53\u7ed3\u6784\u53d1\u751f\u4e86\u90e8\u5206\u53d8\u5316\uff0cSEM\u548cUV-Vis\u5b9e\u9a8c\u663e\u793a\u5176\u5fae\u89c2\u5f62\u8c8c\u548c\u5149\u5b66\u6027\u8d28\u53d1\u751f\u4e86\u5fae\u5f31\u53d8\u5316\u3002\u603b\u4f53\u800c\u8a00\uff0c\u5f02\u8f9b\u9178\u950c\u5728\u4e2d\u6e29\u6761\u4ef6\u4e0b\u4ecd\u5177\u6709\u8f83\u597d\u7684\u7a33\u5b9a\u6027\uff0c\u9002\u5408\u5728\u4e2d\u6e29\u73af\u5883\u4e0b\u5e94\u7528\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u9ad8\u6e29\u533a\uff08200\u00b0C &#8211; 300\u00b0C\uff09<\/strong>\uff1a\u5f53\u6e29\u5ea6\u8d85\u8fc7200\u00b0C\u65f6\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u70ed\u7a33\u5b9a\u6027\u548c\u5316\u5b66\u7a33\u5b9a\u6027\u663e\u8457\u4e0b\u964d\uff0c\u53d1\u751f\u4e86\u5267\u70c8\u7684\u5206\u89e3\u53cd\u5e94\uff0c\u751f\u6210\u4e86\u6c27\u5316\u950c\u548c\u5176\u4ed6\u526f\u4ea7\u7269\u3002DSC\u5b9e\u9a8c\u663e\u793a\uff0c\u5f02\u8f9b\u9178\u950c\u5728\u6b64\u6e29\u5ea6\u533a\u95f4\u5185\u51fa\u73b0\u4e86\u663e\u8457\u7684\u653e\u70ed\u5cf0\uff0cTGA\u5b9e\u9a8c\u8868\u660e\u5176\u5931\u91cd\u7387\u6025\u5267\u589e\u52a0\uff0cFTIR\u548cXRD\u5b9e\u9a8c\u663e\u793a\u5176\u5316\u5b66\u7ed3\u6784\u548c\u6676\u4f53\u7ed3\u6784\u53d1\u751f\u4e86\u663e\u8457\u53d8\u5316\uff0cSEM\u548cUV-Vis\u5b9e\u9a8c\u663e\u793a\u5176\u5fae\u89c2\u5f62\u8c8c\u548c\u5149\u5b66\u6027\u8d28\u53d1\u751f\u4e86\u663e\u8457\u53d8\u5316\u3002\u8fd9\u4e9b\u7ed3\u679c\u8868\u660e\uff0c\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u6761\u4ef6\u4e0b\u4e0d\u9002\u5408\u957f\u671f\u4f7f\u7528\uff0c\u5bb9\u6613\u53d1\u751f\u5206\u89e3\u548c\u5931\u6548\u3002<\/p>\n<\/li>\n<\/ol>\n<p>\u57fa\u4e8e\u4e0a\u8ff0\u5b9e\u9a8c\u7ed3\u679c\uff0c\u53ef\u4ee5\u5f97\u51fa\u4ee5\u4e0b\u51e0\u70b9\u5efa\u8bae\u548c\u5c55\u671b\uff1a<\/p>\n<ol>\n<li>\n<p><strong>\u5e94\u7528\u5efa\u8bae<\/strong>\uff1a\u5f02\u8f9b\u9178\u950c\u5728\u4f4e\u6e29\u548c\u4e2d\u6e29\u6761\u4ef6\u4e0b\u5177\u6709\u826f\u597d\u7684\u7a33\u5b9a\u6027\uff0c\u9002\u7528\u4e8e\u6d82\u6599\u3001\u5851\u6599\u3001\u6a61\u80f6\u3001\u6da6\u6ed1\u5242\u7b49\u884c\u4e1a\u7684\u4f4e\u6e29\u548c\u4e2d\u6e29\u52a0\u5de5\u8fc7\u7a0b\u3002\u7136\u800c\uff0c\u5728\u9ad8\u6e29\u6761\u4ef6\u4e0b\uff0c\u5f02\u8f9b\u9178\u950c\u5bb9\u6613\u53d1\u751f\u5206\u89e3\uff0c\u56e0\u6b64\u5728\u9ad8\u6e29\u5e94\u7528\u4e2d\u5e94\u8c28\u614e\u4f7f\u7528\uff0c\u6216\u8003\u8651\u4f7f\u7528\u5176\u4ed6\u66f4\u4e3a\u7a33\u5b9a\u7684\u66ff\u4ee3\u54c1\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u6539\u6027\u7814\u7a76<\/strong>\uff1a\u4e3a\u4e86\u63d0\u9ad8\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\uff0c\u672a\u6765\u7684\u7814\u7a76\u53ef\u4ee5\u96c6\u4e2d\u5728\u5bf9\u5176\u7ed3\u6784\u8fdb\u884c\u6539\u6027\uff0c\u4f8b\u5982\u5f15\u5165\u5176\u4ed6\u91d1\u5c5e\u79bb\u5b50\u6216\u6709\u673a\u5b98\u80fd\u56e2\uff0c\u4ee5\u589e\u5f3a\u5176\u70ed\u7a33\u5b9a\u6027\u548c\u5316\u5b66\u7a33\u5b9a\u6027\u3002\u6b64\u5916\uff0c\u8fd8\u53ef\u4ee5\u63a2\u7d22\u65b0\u578b\u7684\u5408\u6210\u65b9\u6cd5\uff0c\u5236\u5907\u5177\u6709\u66f4\u9ad8\u7a33\u5b9a\u6027\u7684\u5f02\u8f9b\u9178\u950c\u884d\u751f\u7269\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u673a\u5236\u63a2\u8ba8<\/strong>\uff1a\u5c3d\u7ba1\u672c\u7814\u7a76\u5df2\u7ecf\u63ed\u793a\u4e86\u5f02\u8f9b\u9178\u950c\u5728\u4e0d\u540c\u6e29\u5ea6\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\u53d8\u5316\uff0c\u4f46\u5bf9\u4e8e\u5176\u5206\u89e3\u673a\u5236\u7684\u7406\u89e3\u4ecd\u6709\u5f85\u6df1\u5165\u3002\u672a\u6765\u7684\u7814\u7a76\u53ef\u4ee5\u7ed3\u5408\u7406\u8bba\u8ba1\u7b97\u548c\u5b9e\u9a8c\u9a8c\u8bc1\uff0c\u8fdb\u4e00\u6b65\u63a2\u8ba8\u5f02\u8f9b\u9178\u950c\u5728\u9ad8\u6e29\u6761\u4ef6\u4e0b\u7684\u5206\u89e3\u8def\u5f84\u548c\u53cd\u5e94\u52a8\u529b\u5b66\uff0c\u4e3a\u5f00\u53d1\u66f4\u7a33\u5b9a\u7684\u950c\u5316\u5408\u7269\u63d0\u4f9b\u7406\u8bba\u4f9d\u636e\u3002<\/p>\n<\/li>\n<li>\n<p><strong>\u5b9e\u9645\u5e94\u7528\u9a8c\u8bc1<\/strong>\uff1a\u5b9e\u9a8c\u5ba4\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\u7814\u7a76\u867d\u7136\u63d0\u4f9b\u4e86\u91cd\u8981\u7684\u53c2\u8003\uff0c\u4f46\u5728\u5b9e\u9645\u5de5\u4e1a\u5e94\u7528\u4e2d\uff0c\u5f02\u8f9b\u9178\u950c\u7684\u7a33\u5b9a\u6027\u8fd8\u53d7\u5230\u5176\u4ed6\u56e0\u7d20\u7684\u5f71\u54cd\uff0c\u5982\u6e7f\u5ea6\u3001\u6c14\u6c1b\u3001\u538b\u529b\u7b49\u3002\u56e0\u6b64\uff0c\u672a\u6765\u7684\u7814\u7a76\u53ef\u4ee5\u5728\u66f4\u63a5\u8fd1\u5b9e\u9645\u5e94\u7528\u7684\u6761\u4ef6\u4e0b\u8fdb\u884c\u9a8c\u8bc1\uff0c\u786e\u4fdd\u5176\u5728\u590d\u6742\u73af\u5883\u4e2d\u7684\u957f\u671f\u7a33\u5b9a\u6027\u3002<\/p>\n<\/li>\n<\/ol>\n<p>\u603b\u4e4b\uff0c\u5f02\u8f9b\u9178\u950c\u4f5c\u4e3a\u4e00\u79cd\u91cd\u8981\u7684\u6709\u673a\u950c\u5316\u5408\u7269\uff0c\u5728\u591a\u4e2a\u9886\u57df\u4e2d\u5177\u6709\u5e7f\u6cdb\u7684\u5e94\u7528\u524d\u666f\u3002\u7136\u800c\uff0c\u5176\u5728\u9ad8\u6e29\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\u95ee\u9898\u4e0d\u5bb9\u5ffd\u89c6\u3002\u901a\u8fc7\u6df1\u5165\u7814\u7a76\u5176\u5728\u4e0d\u540c\u6e29\u5ea6\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\u53d8\u5316\uff0c\u53ef\u4ee5\u4e3a\u4f18\u5316\u5176\u5e94\u7528\u63d0\u4f9b\u79d1\u5b66\u4f9d\u636e\uff0c\u5e76\u4e3a\u5f00\u53d1\u66f4\u7a33\u5b9a\u7684\u950c\u5316\u5408\u7269\u5960\u5b9a\u57fa\u7840\u3002<\/p>\n<p>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.bdmaee.net\/cas%ef%bc%9a-2969-81-5\/\">https:\/\/www.bdmaee.net\/cas%ef%bc%9a-2969-81-5\/<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.cyclohexylamine.net\/nn-dicyclohexylmethylamine-cas-7560-83-0-polycat-12\/\">https:\/\/www.cyclohexylamine.net\/nn-dicyclohexylmethylamine-cas-7560-83-0-polycat-12\/<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.cyclohexylamine.net\/semi-hard-foam-catalyst-tmr-3-hard-foam-catalyst-tmr-3\/\">https:\/\/www.cyclohexylamine.net\/semi-hard-foam-catalyst-tmr-3-hard-foam-catalyst-tmr-3\/<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.bdmaee.net\/dabco-pt302-catalyst-cas1739-84-0-evonik-germany\/\">https:\/\/www.bdmaee.net\/dabco-pt302-catalyst-cas1739-84-0-evonik-germany\/<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.bdmaee.net\/n-3-dimethyl-amino-propyl-n-n-diisopropanolamine\/\">https:\/\/www.bdmaee.net\/n-3-dimethyl-amino-propyl-n-n-diisopropanolamine\/<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.newtopchem.com\/archives\/44688\">https:\/\/www.newtopchem.com\/archives\/44688<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.bdmaee.net\/wp-content\/uploads\/2022\/08\/-R-8020-Jeffcat-TD-20-TEDA-A20.pdf\">https:\/\/www.bdmaee.net\/wp-content\/uploads\/2022\/08\/-R-8020-Jeffcat-TD-20-TEDA-A20.pdf<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.bdmaee.net\/delay-catalyst-a-300\/\">https:\/\/www.bdmaee.net\/delay-catalyst-a-300\/<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.newtopchem.com\/archives\/44625\">https:\/\/www.newtopchem.com\/archives\/44625<\/a><\/br><br \/>\u6269\u5c55\u9605\u8bfb:<a href=\"https:\/\/www.bdmaee.net\/lupragen-n500-catalyst-basf\/\">https:\/\/www.bdmaee.net\/lupragen-n500-catalyst-basf\/<\/a><\/br><\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u5f02\u8f9b\u9178\u950c\u7684\u6982\u8ff0\u53ca\u5176\u5e94\u7528\u80cc\u666f \u5f02\u8f9b\u9178\u950c\uff08Zinc 2-Ethylhexanoate\uff09\uff0c\u5316\u5b66\u5f0f\u4e3aZn(C8H15O2)2\uff0c\u662f\u4e00\u79cd\u91cd\u8981\u7684\u6709\u673a\u950c\u5316\u5408\u7269\u3002\u5b83\u7531\u950c\u79bb\u5b50\u548c\u5f02\u8f9b\u9178\u6839\u79bb\u5b50\u7ec4\u6210\uff0c\u5177\u6709\u826f\u597d\u7684\u70ed\u7a33\u5b9a\u6027\u548c\u5316\u5b66\u7a33\u5b9a\u6027\u3002\u5f02\u8f9b\u9178\u950c\u5e7f\u6cdb\u5e94\u7528\u4e8e\u591a\u4e2a\u9886\u57df\uff0c\u7279\u522b\u662f\u5728\u6d82\u6599\u3001\u5851\u6599\u3001\u6a61\u80f6\u3001\u6da6\u6ed1\u5242\u7b49\u884c\u4e1a\u4e2d\uff0c\u4f5c\u4e3a\u50ac\u5316\u5242\u3001\u7a33\u5b9a\u5242\u548c\u9632\u8001\u5242\u7b49\u53d1\u6325\u7740\u91cd\u8981\u4f5c\u7528\u3002 &#8230;<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":[],"categories":[4],"tags":[],"_links":{"self":[{"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/posts\/6409"}],"collection":[{"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/comments?post=6409"}],"version-history":[{"count":0,"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/posts\/6409\/revisions"}],"wp:attachment":[{"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/media?parent=6409"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/categories?post=6409"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.51dmea.cn\/wp-json\/wp\/v2\/tags?post=6409"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}